By Prof. Dr. J. W. Niemantsverdriet(auth.)
“… this publication is a uniquely beneficial consultant to a few of the significant (and a few minor) options used to enquire the buildings of reliable catalysts and version structures and is written from the viewpoint of a prolific researcher within the box. The writing is pleasing to learn, the illustrations are transparent, and the reader is guided successfully to key technical references for additional info… “ –Journal of the yankee Chemical Society
Superbly equipped and of serious pedagogic worth, Spectroscopy in Catalysis describes crucial smooth analytical strategies used to enquire catalytic surfaces. those comprise electron, ion, and vibrational spectroscopy, mass spectrometry, temperature-programmed strategies, diffraction, and microscopy. With the focal point on sensible use, instead of idea, every one bankruptcy provides present functions to demonstrate the kind of details that the approach presents and evaluates its percentages and boundaries, permitting collection of the simplest catalyst and the right kind strategy to resolve a given problem.
This 3rd version comprises major new advancements and case stories, with all of the chapters up to date in terms of contemporary examples and correct new literature. for college students and for everybody who wishes a digestible creation to catalyst characterization.Content:
Chapter 1 creation (pages 1–10):
Chapter 2 Temperature?Programmed thoughts (pages 11–38):
Chapter three Photoemission and Auger Spectroscopy (pages 39–83):
Chapter four The Ion Spectroscopies (pages 85–119):
Chapter five Mossbauer Spectroscopy (pages 121–146):
Chapter 6 Diffraction and prolonged X?Ray Absorption wonderful constitution (EXAFS) (pages 147–177):
Chapter 7 Microscopy and Imaging (pages 179–216):
Chapter eight Vibrational Spectroscopy (pages 217–249):
Chapter nine Case reports in Catalyst Characterization (pages 251–295):
Read or Download Spectroscopy in Catalysis: An Introduction, Third Edition PDF
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Additional resources for Spectroscopy in Catalysis: An Introduction, Third Edition
02 10 12 10 13 10 14 3 Á 10 17 10 13 V Cr Mn Fe Co Ni Cu Mo Ru Rh Pd Ag Ir equilibrium value and the eﬃciency with which water is removed from the reactor becomes the decisive factor. 2 provides a complete phase diagram for the reduction of iron oxide at diﬀerent temperatures [3, 5]. In order to reduce bulk iron oxide to metallic iron at 600 K, the water content of the hydrogen gas above the sample must be below a few percent, which is easily achieved. However, in order to reduce Cr2 O3 , the water content should be as low as a few parts per billion, which is much more diﬃcult to realize.
This led to a technique called electron spectroscopy for chemical analysis (ESCA), which today is more commonly referred to as X-ray photoelectron spectroscopy (XPS) Spectroscopy in Catalysis: An Introduction, Third Edition J. W. Niemantsverdriet Copyright 8 2007 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim ISBN: 978-3-527-31651-9 40 3 Photoemission and Auger Spectroscopy . Commercial instruments of this type have been available since the early 1970s, and in 1981 Siegbahn received the Nobel Prize for his eﬀorts in the ﬁeld.
15), and a faster reaction channel for desorption opens up, as seen by the development of a shoulder at lower temperatures . 9 corresponds to the recombinative desorption of N-atoms on Rh(100). As two adsorbed N-atoms are involved, the rate of desorption depends on the coverage squared; this leads to TPD peaks which shift to lower temperatures with increasing coverage . The presence of lateral interactions is diﬃcult to recognize without detailed analysis of the kinetics (this point is discussed later).