Anisotropy in Single-Crystal Refractory Compounds: by Bertil Aronsson, Torsten Lundström, Ingvar Engström (auth.),

By Bertil Aronsson, Torsten Lundström, Ingvar Engström (auth.), Fred W. Vahldiek, Stanley A. Mersol (eds.)

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Extra info for Anisotropy in Single-Crystal Refractory Compounds: Proceedings of an International Symposium on Anisotropy in Single-Crystal Refractory Compounds, held on June 13–15, 1967, in Dayton Ohio. Sponsored by the Ceramics and Branch of the air Force Materials La

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26 CRYSTAL STRUCTURE AND CHEMISTRY 60 PLATEAU -ao----- •• '. '• It j,... ----(- • • ,. Fig. 2. Mo distribution, single crystal MozC, C-l, plateau. ---- -'"-- S. H. MOLL AND G. W. BRUNO 27 The monochromator crystal now utilized is an artificially formed lead stearate decanoate overlay formed on a suitable substrate. The x-ray detector is a traditional gas flow proportional counter utilizing a thin formvar or collodion window to separate the detector gas from the vacuum x-ray path. Gas mixtures used include various methane/argon mixtures at atmospheric or less than atmospheric pressure.

1S ) (2) With increasing group number of the metal, Me-B distances tend to become shorter, whereas Me-Me and B-B distances become longer. The structure proposed for WB4 as well as the explanations of the extended homogeneity ranges of NbB2, WB2 and M02BS are consistent with the first observation. Accordingly, they appear more likely than earlier suggestions. In particular, it does not seem probable that f-layers of boron exist at all. For WB2 this has been shown by the experimental results quoted above; the high boron content of M02BS may depend on a Mo-B2 "substitution" of the type envisaged for NbB2 rather than on the presence of f-layers as claimed earlier.

8 Fig. 6. MozC crystal (C-9), longitudinal surface, 606 x. _~. •• V ~_ _ U ... t . ,.. ' ,,~ ... ,.. ~ 'W: ~_ ~L • 't ~~.... _ : .. \4 3 w/o / B-2 0 Fig. 7. Ta distribution, single crystal MozC, C-8 (CS), edge. _V V. ...... • ;; 60 __ 7Q~ _ _ _ _ 50 _. __ . < :...... - _ _ - _ . I ,! __ 2 _____ ~. l _ _ _ _ _ _ . -/ hU <&r

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